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PharmLabs San Diego Certificate of Analysis
Sample Pharma Hemp Suppository 25mg
Delta9 THC 0.02% THCa ND Total THC (THC + THCa) 0.02%
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Sample ID  SD181012-015 (30718) Matrix   Other (Other Cannabis Good)  Batch ID/Lot ID  O3-1
Tested for  MCNB Holding Corporation
Sampled   - Received   Oct 12, 2018 Reported   Oct 19, 2018
Analyses executed   CAN, TER, MIBNIG, PES Unit Mass (g)   2.215

CAN - Cannabinoids

Analyzed Oct 16, 2018  |  Instrument HPLC-VWD  | Method SOP-001
The expanded Uncertainty of the Cannabinoid analysis is approximately ±7.806% at the 95% Confidence Level
Analyte   LOD
mg/g 		LOQ
mg/g 		Result
% 		Result
mg/g		 Result
mg/Unit
Cannabidiolic Acid (CBDA)   0.001 0.16 0.00 0.01 0.02
Cannabigerol (CBG)   0.001 0.16 ND ND ND
Cannabidiol (CBD)   0.001 0.16 1.07 10.71 23.72
Cannabinol (CBN)   0.001 0.16 ND ND ND
Tetrahydrocannabinol (Δ9-THC)   0.003 0.16 0.00 0.02 0.04
Δ8-tetrahydrocannabinol (Δ8-THC)   0.004 0.16 NT NT NT
(6aR,9S)-Δ10-Tetrahydrocannabinol ((6aR,9S)-Δ10)   0.015 0.16 NT NT NT
(6aR,9R)-Δ10-Tetrahydrocannabinol ((6aR,9R)-Δ10)   0.007 0.16 NT NT NT
Tetrahydrocannabinolic Acid (THCA)   0.001 0.16 ND ND ND
Total THC ( THCa * 0.877 + Δ9THC )       0.00 0.02 0.04
Total CBD ( CBDa * 0.877 + CBD )       1.07 10.72 23.74
Total Cannabinoids Analyzed       1.07 10.74 23.79

MIBNIG - Microbial

Analyzed Oct 18, 2018  |  Instrument Plating  | Method SOP-007
Analyte LOD
 LOQ
 Result
CFU/g 		Limit Analyte LOD
 LOQ
 Result
CFU/g 		Limit
Shiga toxin-producing Escherichia Coli Negative ND per 1 gram Salmonella spp. Negative ND per 1 gram

PES - Pesticides

Analyzed Oct 18, 2018  |  Instrument LC/MSMS GC/MSMS  | Method SOP-003
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Aldicarb 0.0078 0.02 ND 0.0078 Carbofuran 0.01 0.02 ND 0.01
Dimethoate 0.01 0.02 ND 0.01 Etofenprox 0.02 0.1 ND 0.02
Fenoxycarb 0.01 0.02 ND 0.01 Thiachloprid 0.01 0.02 ND 0.01
Daminozide 0.01 0.03 ND 0.01 Dichlorvos 0.02 0.07 ND 0.02
Imazalil 0.02 0.07 ND 0.02 Methiocarb 0.01 0.02 ND 0.01
Spiroxamine 0.01 0.02 ND 0.01 Coumaphos 0.01 0.02 ND 0.01
Fipronil 0.01 0.1 ND 0.01 Paclobutrazol 0.01 0.03 ND 0.01
Chlorpyrifos 0.01 0.04 ND 0.01 Ethoprophos (Prophos) 0.01 0.02 ND 0.01
Baygon (Propoxur) 0.01 0.02 ND 0.01 Chlordane 0.04 0.1 ND 0.04
Chlorfenapyr 0.03 0.1 ND 0.03 Methyl Parathion 0.02 0.1 ND 0.02
Mevinphos 0.03 0.08 ND 0.03 Abamectin 0.03 0.08 ND 0.3
Acephate 0.02 0.05 ND 5 Acetamiprid 0.01 0.05 ND 5
Azoxystrobin 0.01 0.02 ND 40 Bifenazate 0.01 0.05 ND 5
Bifenthrin 0.02 0.35 ND 0.5 Boscalid 0.01 0.03 ND 10
Carbaryl 0.01 0.02 ND 0.5 Chlorantraniliprole 0.01 0.04 ND 40
Clofentezine 0.01 0.03 ND 0.5 Diazinon 0.01 0.02 ND 0.2
Dimethomorph 0.02 0.06 ND 20 Etoxazole 0.01 0.05 ND 1.5
Fenpyroximate 0.02 0.1 ND 2 Flonicamid 0.01 0.02 ND 2
Fludioxonil 0.01 0.05 ND 30 Hexythiazox 0.01 0.03 ND 2
Imidacloprid 0.01 0.05 ND 3 Kresoxim-methyl 0.01 0.03 ND 1
Malathion 0.01 0.05 ND 5 Metalaxyl 0.01 0.02 ND 15
Methomyl 0.02 0.05 ND 0.1 Myclobutanil 0.02 0.07 ND 9
Naled 0.01 0.02 ND 0.5 Oxamyl 0.01 0.02 ND 0.2
Permethrin 0.01 0.02 ND 20 Phosmet 0.01 0.02 ND 0.2
Piperonyl Butoxide 0.02 0.06 ND 8 Propiconazole 0.03 0.08 ND 20
Prallethrin 0.02 0.05 ND 0.4 Pyrethrin 0.05 0.41 ND 1
Pyridaben 0.02 0.07 ND 3 Spinosad A 0.01 0.05 ND 3
Spinosad D 0.01 0.05 ND 3 Spiromesifen 0.02 0.06 ND 12
Spirotetramat 0.01 0.02 ND 13 Tebuconazole 0.01 0.02 ND 2
Thiamethoxam 0.01 0.02 ND 4.5 Trifloxystrobin 0.01 0.02 ND 30
Acequinocyl 0.02 0.09 ND 4 Captan 0.01 0.02 ND 5
Cypermethrin 0.02 0.1 ND 1 Cyfluthrin 0.04 0.1 ND 1
Fenhexamid 0.02 0.07 ND 10 Spinetoram J,L 0.02 0.07 ND 3
Pentachloronitrobenzene 0.01 0.1 ND 0.2  

TER - Terpenes

Analyzed Oct 18, 2018  |  Instrument GC/FID  | Method SOP-002
Analyte LOD
mg/g 		LOQ
mg/g 		(%) (mg/g) Analyte LOD
mg/g 		LOQ
mg/g 		(%) (mg/g)
a-Pinene (a-Pin) 0.128 0.427 0.06 0.55 Camphene (Cam) 0.147 0.492 ND ND
Myrcene (Myr) 0.073 0.244 0.01 0.06 b-Pinene (b-Pin) 0.413 1.377 0.00 0.03
3-Carene (3-Car) 0.11 0.366 0.03 0.29 a-Terpinene (a-Ter) 0.099 0.331 0.01 0.12
a-Ocimene (a-Oci) 0.055 0.182 0.00 0.02 Limonene (Lim) 0.081 0.268 0.01 0.14
p-Cymene (p-Cym) 0.104 0.347 0.01 0.13 b-Ocimene (b-Oci) 0.085 0.282 0.01 0.06
Eucalyptol (Euc) 0.19 0.634 ND ND g-Terpinene (g-Ter) 0.108 0.361 0.02 0.22
Terpenolene (Terp) 0.119 0.395 0.01 0.05 Linalool (Lin) 0.146 0.487 ND ND
Isopulegol (Isop) 0.139 0.464 ND ND Geraniol (Gera) 0.177 0.589 ND ND
b-Caryophyllene (b-Cary) 0.132 0.44 ND ND a-Humulene (Hum) 0.183 0.608 ND ND
cis-Nerolidol (ci-Ner) 0.129 0.431 ND ND trans-Nerolidol (tr-Ner) 0.093 0.31 ND ND
Guaiol (Gua) 0.15 0.499 ND ND Caryophyllene Oxide (CarOx) 0.183 0.611 ND ND
a-bisabolol (a-Bbis) 0.159 0.529 ND ND  
  Total Terpene Concentration   0.17 % 1.67 mg/g

Terpene Testing - Visualization

Terpene Chart Loading