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PharmLabs San Diego Certificate of Analysis
Sample 804A
Delta9 THC ND THCa ND Total THC (THC + THCa) ND Delta8 THC 87.80%
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Sample ID  SD200918-012 (39421) Matrix   Distillate - NI (Other Cannabis Good)
Tested for  Recreational 8
Sampled   - Received   Sep 18, 2020 Reported   Sep 28, 2020
Analyses executed   CAN+, RES, MIBIG, MTO, PES, HME, FVI

CAN+ - Cannabinoids

Analyzed Sep 19, 2020  |  Instrument HPLC-VWD  | Method SOP-001
The expanded Uncertainty of the Cannabinoid analysis is approximately ±7.806% at the 95% Confidence Level
Analyte   LOD
mg/g 		LOQ
mg/g 		Result
% 		Result
mg/g
Cannabidivarin (CBDV)   0.039 0.16 ND ND
Cannabidiolic Acid (CBDA)   0.001 0.16 ND ND
Cannabigerol Acid (CBGA)   0.001 0.16 ND ND
Cannabigerol (CBG)   0.001 0.16 ND ND
Cannabidiol (CBD)   0.001 0.16 ND ND
Tetrahydrocannabivarin (THCV)   0.001 0.16 ND ND
Cannabinol (CBN)   0.001 0.16 <LOQ <LOQ
Tetrahydrocannabinol (Δ9-THC)   0.003 0.16 ND ND
Δ8-tetrahydrocannabinol (Δ8-THC)   0.004 0.16 87.80 878.05
Cannabicyclol (CBL)   0.002 0.16 ND ND
Cannabichromene (CBC)   0.002 0.16 ND ND
Tetrahydrocannabinolic Acid (THCA)   0.001 0.16 ND ND
Total THC ( THCa * 0.877 + Δ9THC )       ND ND
Total THC + Δ8THC ( THCa * 0.877 + Δ9THC + Δ8THC )       87.80 878.05
Total CBD ( CBDa * 0.877 + CBD )       ND ND
Total CBG ( CBGa * 0.877 + CBG )       ND ND
Total Cannabinoids Analyzed       87.80 878.05

HME - Heavy Metals

Analyzed Sep 28, 2020  |  Instrument ICP/MSMS  | Method SOP-005
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Arsenic (As) 0.0009 0.0027 ND 1.5
Cadmium (Cd) 0.0005 0.0015 ND 0.5
Mercury (Hg) 0.0058 0.0174 0.05 3
Lead (Pb) 0.0006 0.0018 0.01 0.5
Nickel (Ni) 6.0e-05 0.0002 NT

MIBIG - Microbial

Analyzed Sep 24, 2020  |  Instrument qPCR and/or Plating  | Method SOP-007
Analyte LOD
 LOQ
 Result
CFU/g 		Limit Analyte LOD
 LOQ
 Result
CFU/g 		Limit
Shiga toxin-producing Escherichia Coli Negative ND per 1 gram Salmonella spp. Negative ND per 1 gram
Aspergillus fumigatus Negative ND per 1 gram Aspergillus flavus Negative ND per 1 gram
Aspergillus niger Negative ND per 1 gram Aspergillus terreus Negative ND per 1 gram

MTO - Mycotoxin

Analyzed Sep 25, 2020  |  Instrument LC/MSMS  | Method SOP-004
Analyte LOD
ug/kg 		LOQ
ug/kg 		Result
ug/kg (ppb) 		Limit
ug/kg 		Analyte LOD
ug/kg 		LOQ
ug/kg 		Result
ug/kg (ppb) 		Limit
ug/kg
Ochratoxin A 5.0 20.0 ND 20 Aflatoxin B1 2.5 5.0 ND -
Aflatoxin B2 2.5 5.0 ND - Aflatoxin G1 2.5 5.0 ND -
Aflatoxin G2 2.5 5.0 ND - Total Aflatoxins 10.0 20.0 ND 20

PES - Pesticides

Analyzed Sep 25, 2020  |  Instrument LC/MSMS GC/MSMS  | Method SOP-003
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Aldicarb 0.0078 0.02 ND 0.0078 Carbofuran 0.01 0.02 ND 0.01
Dimethoate 0.01 0.02 ND 0.01 Etofenprox 0.02 0.1 ND 0.02
Fenoxycarb 0.01 0.02 ND 0.01 Thiachloprid 0.01 0.02 ND 0.01
Daminozide 0.01 0.03 ND 0.01 Dichlorvos 0.02 0.07 ND 0.02
Imazalil 0.02 0.07 ND 0.02 Methiocarb 0.01 0.02 ND 0.01
Spiroxamine 0.01 0.02 ND 0.01 Coumaphos 0.01 0.02 ND 0.01
Fipronil 0.01 0.1 ND 0.01 Paclobutrazol 0.01 0.03 ND 0.01
Chlorpyrifos 0.01 0.04 ND 0.01 Ethoprophos (Prophos) 0.01 0.02 ND 0.01
Baygon (Propoxur) 0.01 0.02 ND 0.01 Chlordane 0.04 0.1 ND 0.04
Chlorfenapyr 0.03 0.1 ND 0.03 Methyl Parathion 0.02 0.1 ND 0.02
Mevinphos 0.03 0.08 ND 0.03 Abamectin 0.03 0.08 ND 0.3
Acephate 0.02 0.05 ND 5 Acetamiprid 0.01 0.05 ND 5
Azoxystrobin 0.01 0.02 ND 40 Bifenazate 0.01 0.05 ND 5
Bifenthrin 0.02 0.35 ND 0.5 Boscalid 0.01 0.03 ND 10
Carbaryl 0.01 0.02 ND 0.5 Chlorantraniliprole 0.01 0.04 ND 40
Clofentezine 0.01 0.03 ND 0.5 Diazinon 0.01 0.02 ND 0.2
Dimethomorph 0.02 0.06 ND 20 Etoxazole 0.01 0.05 ND 1.5
Fenpyroximate 0.02 0.1 ND 2 Flonicamid 0.01 0.02 ND 2
Fludioxonil 0.01 0.05 ND 30 Hexythiazox 0.01 0.03 ND 2
Imidacloprid 0.01 0.05 ND 3 Kresoxim-methyl 0.01 0.03 ND 1
Malathion 0.01 0.05 ND 5 Metalaxyl 0.01 0.02 ND 15
Methomyl 0.02 0.05 ND 0.1 Myclobutanil 0.02 0.07 ND 9
Naled 0.01 0.02 ND 0.5 Oxamyl 0.01 0.02 ND 0.2
Permethrin 0.01 0.02 ND 20 Phosmet 0.01 0.02 ND 0.2
Piperonyl Butoxide 0.02 0.06 ND 8 Propiconazole 0.03 0.08 ND 20
Prallethrin 0.02 0.05 ND 0.4 Pyrethrin 0.05 0.41 ND 1
Pyridaben 0.02 0.07 ND 3 Spinosad A 0.01 0.05 ND 3
Spinosad D 0.01 0.05 ND 3 Spiromesifen 0.02 0.06 ND 12
Spirotetramat 0.01 0.02 ND 13 Tebuconazole 0.01 0.02 ND 2
Thiamethoxam 0.01 0.02 ND 4.5 Trifloxystrobin 0.01 0.02 ND 30
Acequinocyl 0.02 0.09 ND 4 Captan 0.01 0.02 ND 5
Cypermethrin 0.02 0.1 ND 1 Cyfluthrin 0.04 0.1 ND 1
Fenhexamid 0.02 0.07 ND 10 Spinetoram J,L 0.02 0.07 ND 3
Pentachloronitrobenzene 0.01 0.1 ND 0.2  

RES - Residual Solvents

Analyzed Sep 23, 2020  |  Instrument GC/FID with Headspace Analyzer  | Method SOP-006
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Propane (Prop) 0.4 40.0 ND 5000 Butane (But) 0.4 40.0 <LOQ 5000
Methanol (Metha) 0.4 40.0 <LOQ 3000 Ethylene Oxide (EthOx) 0.4 0.8 ND 1
Pentane (Pen) 0.4 40.0 ND 5000 Ethanol (Ethan) 0.4 40.0 ND 5000
Ethyl Ether (EthEt) 0.4 40.0 ND 5000 Acetone (Acet) 0.4 40.0 <LOQ 5000
Isopropanol (2-Pro) 0.4 40.0 <LOQ 5000 Acetonitrile (Acetonit) 0.4 40.0 <LOQ 410
Methylene Chloride (MetCh) 0.4 0.8 ND 1 Hexane (Hex) 0.4 40.0 ND 290
Ethyl Acetate (EthAc) 0.4 40.0 ND 5000 Chloroform (Clo) 0.4 0.8 ND 1
Benzene (Ben) 0.4 0.8 ND 1 1-2-Dichloroethane (12-Dich) 0.4 0.8 ND 1
Heptane (Hep) 0.4 40.0 ND 5000 Trichloroethylene (TriClEth) 0.4 0.8 ND 1
Toluene (Toluene) 0.4 40.0 ND 890 Xylenes (Xyl) 0.4 40.0 NT 2170

FVI - Filth & Foreign Material Inspection

Analyzed Sep 23, 2020  |  Instrument Microscope  | Method SOP-010
Analyte / Limit Result
 Analyte / Limit Result
> 1/4 of the total sample area
covered by sand, soil, cinders, or dirt 		Negative > 1/4 of the total sample area
covered by mold 		Negative
> 1 insect fragment, 1 hair, or 1 count
mammalian excreta per 3g 		Negative > 1/4 of the total sample area
covered by an imbedded foreign material 		Negative