QA Testing

download/print PDF version
reload without photo
PharmLabs San Diego Certificate of Analysis
Sample Smilyn D8 Candy Clusters Blue Razz Retest
Delta9 THC 0.58% THCa ND Total THC (THC + THCa) 0.58% Delta8 THC 4.33%
Logo_coa
Sample ID  SD220901-086 (51187) Matrix   Edible (Other Cannabis Good)
Tested for  Cabo Ella Group DBA Smilyn Wellness
Sampled   - Received   Aug 01, 2022 Reported   Oct 04, 2022
Analyses executed   CAN+, RES, MIBNIG, PES, HME, FVI, MWA Unit Mass (g)   13.731 Serving Size (g)   0.34

Laboratory note: unit size = 10 pieces | serving = 1/4 of a gummy bite

CAN+ - Cannabinoids

Analyzed Aug 09, 2022  |  Instrument HPLC-VWD  | Method SOP-001
The expanded Uncertainty of the Cannabinoid analysis is approximately ±7.806% at the 95% Confidence Level
Analyte   LOD
mg/g 		LOQ
mg/g 		Result
% 		Result
mg/g		 Result
mg/Serving		 Result
mg/Unit
Cannabidivarin (CBDV)   0.039 0.16 ND ND ND ND
Cannabidiolic Acid (CBDA)   0.001 0.16 ND ND ND ND
Cannabigerol Acid (CBGA)   0.001 0.16 ND ND ND ND
Cannabigerol (CBG)   0.001 0.16 ND ND ND ND
Cannabidiol (CBD)   0.001 0.16 ND ND ND ND
Tetrahydrocannabivarin (THCV)   0.001 0.16 ND ND ND ND
Cannabinol (CBN)   0.001 0.16 ND ND ND ND
Tetrahydrocannabinol (Δ9-THC)   0.003 0.16 0.06 0.58 0.20 7.98
Δ8-tetrahydrocannabinol (Δ8-THC)   0.004 0.16 0.43 4.33 1.47 59.40
Cannabicyclol (CBL)   0.002 0.16 ND ND ND ND
Cannabichromene (CBC)   0.002 0.16 ND ND ND ND
Tetrahydrocannabinolic Acid (THCA)   0.001 0.16 ND ND ND ND
Total THC ( THCa * 0.877 + Δ9THC )       0.06 0.58 0.20 7.98
Total THC + Δ8THC ( THCa * 0.877 + Δ9THC + Δ8THC )       0.49 4.91 1.67 67.38
Total CBD ( CBDa * 0.877 + CBD )       ND ND ND ND
Total CBG ( CBGa * 0.877 + CBG )       ND ND ND ND
Total Cannabinoids Analyzed       0.49 4.91 1.67 67.38

HME - Heavy Metals

Analyzed Aug 17, 2022  |  Instrument ICP/MSMS  | Method SOP-005
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Arsenic (As) 0.0009 0.0027 ND 1.5
Cadmium (Cd) 0.0005 0.0015 ND 0.5
Mercury (Hg) 0.0058 0.0174 ND 3
Lead (Pb) 0.0006 0.0018 ND 0.5

MIBNIG - Microbial

Analyzed Aug 17, 2022  |  Instrument Plating  | Method SOP-007
Analyte LOD
 LOQ
 Result
CFU/g 		Limit Analyte LOD
 LOQ
 Result
CFU/g 		Limit
Shiga toxin-producing Escherichia Coli ND ND per 1 gram Salmonella spp. ND ND per 1 gram

PES - Pesticides

Analyzed Aug 17, 2022  |  Instrument LC/MSMS GC/MSMS  | Method SOP-003
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Aldicarb 0.0078 0.02 ND 0.0078 Carbofuran 0.01 0.02 ND 0.01
Dimethoate 0.01 0.02 ND 0.01 Etofenprox 0.02 0.1 ND 0.02
Fenoxycarb 0.01 0.02 ND 0.01 Thiachloprid 0.01 0.02 ND 0.01
Daminozide 0.01 0.03 ND 0.01 Dichlorvos 0.02 0.07 ND 0.02
Imazalil 0.02 0.07 ND 0.02 Methiocarb 0.01 0.02 ND 0.01
Spiroxamine 0.01 0.02 ND 0.01 Coumaphos 0.01 0.02 ND 0.01
Fipronil 0.01 0.1 ND 0.01 Paclobutrazol 0.01 0.03 ND 0.01
Chlorpyrifos 0.01 0.04 ND 0.01 Ethoprophos (Prophos) 0.01 0.02 ND 0.01
Baygon (Propoxur) 0.01 0.02 ND 0.01 Chlordane 0.04 0.1 ND 0.04
Chlorfenapyr 0.03 0.1 ND 0.03 Methyl Parathion 0.02 0.1 ND 0.02
Mevinphos 0.03 0.08 ND 0.03 Abamectin 0.03 0.08 ND 0.3
Acephate 0.02 0.05 ND 5 Acetamiprid 0.01 0.05 ND 5
Azoxystrobin 0.01 0.02 ND 40 Bifenazate 0.01 0.05 ND 5
Bifenthrin 0.02 0.35 ND 0.5 Boscalid 0.01 0.03 ND 10
Carbaryl 0.01 0.02 ND 0.5 Chlorantraniliprole 0.01 0.04 ND 40
Clofentezine 0.01 0.03 ND 0.5 Diazinon 0.01 0.02 ND 0.2
Dimethomorph 0.02 0.06 ND 20 Etoxazole 0.01 0.05 ND 1.5
Fenpyroximate 0.02 0.1 ND 2 Flonicamid 0.01 0.02 ND 2
Fludioxonil 0.01 0.05 ND 30 Hexythiazox 0.01 0.03 ND 2
Imidacloprid 0.01 0.05 ND 3 Kresoxim-methyl 0.01 0.03 ND 1
Malathion 0.01 0.05 ND 5 Metalaxyl 0.01 0.02 ND 15
Methomyl 0.02 0.05 ND 0.1 Myclobutanil 0.02 0.07 ND 9
Naled 0.01 0.02 ND 0.5 Oxamyl 0.01 0.02 ND 0.2
Permethrin 0.01 0.02 ND 20 Phosmet 0.01 0.02 ND 0.2
Piperonyl Butoxide 0.02 0.06 ND 8 Propiconazole 0.03 0.08 ND 20
Prallethrin 0.02 0.05 ND 0.4 Pyrethrin 0.05 0.41 ND 1
Pyridaben 0.02 0.07 ND 3 Spinosad A 0.01 0.05 ND 3
Spinosad D 0.01 0.05 ND 3 Spiromesifen 0.02 0.06 ND 12
Spirotetramat 0.01 0.02 ND 13 Tebuconazole 0.01 0.02 ND 2
Thiamethoxam 0.01 0.02 ND 4.5 Trifloxystrobin 0.01 0.02 ND 30
Acequinocyl 0.02 0.09 ND 4 Captan 0.01 0.02 ND 5
Cypermethrin 0.02 0.1 ND 1 Cyfluthrin 0.04 0.1 ND 1
Fenhexamid 0.02 0.07 ND 10 Spinetoram J,L 0.02 0.07 ND 3
Pentachloronitrobenzene 0.01 0.1 ND 0.2  

RES - Residual Solvents

Analyzed Aug 17, 2022  |  Instrument GC/FID with Headspace Analyzer  | Method SOP-006
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Propane (Prop) 0.4 40.0 ND 5000 Butane (But) 0.4 40.0 ND 5000
Methanol (Metha) 0.4 40.0 ND 3000 Ethylene Oxide (EthOx) 0.4 0.8 ND 1
Pentane (Pen) 0.4 40.0 ND 5000 Ethanol (Ethan) 0.4 40.0 ND 5000
Ethyl Ether (EthEt) 0.4 40.0 ND 5000 Acetone (Acet) 0.4 40.0 ND 5000
Isopropanol (2-Pro) 0.4 40.0 ND 5000 Acetonitrile (Acetonit) 0.4 40.0 ND 410
Methylene Chloride (MetCh) 0.4 0.8 ND 1 Hexane (Hex) 0.4 40.0 ND 290
Ethyl Acetate (EthAc) 0.4 40.0 49.2 5000 Chloroform (Clo) 0.4 0.8 ND 1
Benzene (Ben) 0.4 0.8 ND 1 1-2-Dichloroethane (12-Dich) 0.4 0.8 ND 1
Heptane (Hep) 0.4 40.0 ND 5000 Trichloroethylene (TriClEth) 0.4 0.8 ND 1
Toluene (Toluene) 0.4 40.0 ND 890 Xylenes (Xyl) 0.4 40.0 ND 2170

FVI - Filth & Foreign Material Inspection

Analyzed Aug 17, 2022  |  Instrument Microscope  | Method SOP-010
Analyte / Limit Result
 Analyte / Limit Result
> 1/4 of the total sample area
covered by sand, soil, cinders, or dirt 		ND > 1/4 of the total sample area
covered by mold 		ND
> 1 insect fragment, 1 hair, or 1 count
mammalian excreta per 3g 		ND > 1/4 of the total sample area
covered by an imbedded foreign material 		ND

MWA - Moisture Content & Water Activity

Analyzed Aug 17, 2022  |  Instrument Chilled-mirror Dewpoint and Capacitance  | Method SOP-008
Analyte LOD
% 		LOQ
% 		Result
 Limit Analyte LOD
% 		LOQ
% 		Result
 Limit
Moisture (Moi) 0.0 0.0 10.8 % Mw 13 % Mw Water Activity (WA) 0.03 0.03 0.68 aw 0.85 aw