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PharmLabs San Diego
Certificate of Analysis
Sample
Hemp Derived D9 THC
Delta9 THC
82.60%
THCa
ND
Total THC (THCa * 0.877 + THC)
82.60%
Delta8 THC
9.82%
| Sample ID SD220823-010 (51358) | Matrix Concentrate |
| Tested for (763) 260-1696 | Splitrock Farms | ||
| Cultivator/Manufacturer/Microbusiness License 20210971 | Address 14165 James Rd Ste 113 Rogers, MN 55374 | (763) 260-1696 | Name SPLITROCK LABORATORIES |
| Sampled - | Received Aug 22, 2022 | Reported Sep 01, 2022 |
| Analyses executed CAN+, RES, MIBIG, MTO, PES, HME, FVI | |||||
CAN+ - Cannabinoids
Analyzed Sep 01, 2022 | Instrument HPLC-VWD | Method SOP-001The expanded Uncertainty of the Cannabinoids analysis is approximately ± 7.81% at the 95% Confidence Level
| Analyte |
LOD mg/g |
LOQ mg/g |
Result % |
Result mg/g |
|
|---|---|---|---|---|---|
| Cannabidivarin (CBDV) | 0.039 | 0.16 | ND | ND | |
| Cannabidibutol (CBDb) | 0.011 | 0.03 | NT | NT | |
| Cannabidiolic Acid (CBDA) | 0.033 | 0.16 | ND | ND | |
| Cannabigerol Acid (CBGA) | 0.033 | 0.16 | ND | ND | |
| Cannabigerol (CBG) | 0.048 | 0.16 | 0.27 | 2.70 | |
| Cannabidiol (CBD) | 0.069 | 0.229 | 0.40 | 4.00 | |
| Tetrahydrocannabivarin (THCV) | 0.049 | 0.16 | 0.95 | 9.49 | |
| Cannabinol (CBN) | 0.047 | 0.16 | 0.28 | 2.77 | |
| Tetrahydrocannabinol (Δ9-THC) | 0.092 | 0.307 | 82.60 | 825.96 | |
| Δ8-tetrahydrocannabinol (Δ8-THC) | 0.044 | 0.16 | 9.82 | 98.18 | |
| Cannabicyclol (CBL) | 0.0012 | 0.16 | ND | ND | |
| Cannabichromene (CBC) | 0.13 | 0.432 | ND | ND | |
| Tetrahydrocannabinolic Acid (THCA) | 0.117 | 0.389 | ND | ND | |
| Total THC ( THCa * 0.877 + Δ9THC ) | 82.60 | 825.96 | |||
| Total THC + Δ8THC ( THCa * 0.877 + Δ9THC + Δ8THC ) | 92.41 | 924.15 | |||
| Total CBD ( CBDa * 0.877 + CBD ) | 0.40 | 4.00 | |||
| Total CBG ( CBGa * 0.877 + CBG ) | 0.27 | 2.70 | |||
| Total Cannabinoids Analyzed | 94.31 | 943.10 |
HME - Heavy Metals
Analyzed Aug 29, 2022 | Instrument ICP/MSMS | Method SOP-005| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|
| Arsenic (As) | 0.0009 | 0.0027 | <LOQ | 1.5 |
| Cadmium (Cd) | 0.0005 | 0.0015 | <LOQ | 0.5 |
| Mercury (Hg) | 0.0058 | 0.0174 | ND | 3 |
| Lead (Pb) | 0.0006 | 0.0018 | <LOQ | 0.5 |
| Nickel (Ni) | 6.0e-05 | 0.0002 | NT |
MIBIG - Microbial
Analyzed Aug 29, 2022 | Instrument qPCR and/or Plating | Method SOP-007| Analyte |
LOD CFU/g |
LOQ CFU/g |
Result CFU/g |
Limit CFU/g |
|---|---|---|---|---|
| Shiga toxin-producing Escherichia Coli | 1.0 | 1.0 | ND | 1 |
| Salmonella spp. | 1.0 | 1.0 | ND | 1 |
| Aspergillus fumigatus | 1.0 | 1.0 | ND | 1 |
| Aspergillus flavus | 1.0 | 1.0 | ND | 1 |
| Aspergillus niger | 1.0 | 1.0 | ND | 1 |
| Aspergillus terreus | 1.0 | 1.0 | ND | 1 |
MTO - Mycotoxin
Analyzed Aug 31, 2022 | Instrument LC/MSMS | Method SOP-004| Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
|---|---|---|---|---|---|---|---|---|---|
| Ochratoxin A | 5.0 | 20.0 | ND | 20 | Aflatoxin B1 | 2.5 | 5.0 | ND | - |
| Aflatoxin B2 | 2.5 | 5.0 | ND | - | Aflatoxin G1 | 2.5 | 5.0 | ND | - |
| Aflatoxin G2 | 2.5 | 5.0 | ND | - | Total Aflatoxins | 10.0 | 20.0 | ND | 20 |
PES - Pesticides
Analyzed Aug 31, 2022 | Instrument LC/MSMS GC/MSMS | Method SOP-003| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Aldicarb | 0.01 | 0.02 | ND | Carbofuran | 0.01 | 0.02 | ND | ||
| Dimethoate | 0.01 | 0.02 | ND | Etofenprox | 0.02 | 0.1 | ND | ||
| Fenoxycarb | 0.01 | 0.02 | ND | Thiachloprid | 0.01 | 0.02 | ND | ||
| Daminozide | 0.01 | 0.03 | ND | Dichlorvos | 0.02 | 0.07 | ND | ||
| Imazalil | 0.02 | 0.07 | ND | Methiocarb | 0.01 | 0.02 | ND | ||
| Spiroxamine | 0.01 | 0.02 | ND | Coumaphos | 0.01 | 0.02 | ND | ||
| Fipronil | 0.01 | 0.1 | ND | Paclobutrazol | 0.01 | 0.03 | ND | ||
| Chlorpyrifos | 0.01 | 0.04 | ND | Ethoprophos (Prophos) | 0.01 | 0.02 | ND | ||
| Baygon (Propoxur) | 0.01 | 0.02 | ND | Chlordane | 0.04 | 0.1 | ND | ||
| Chlorfenapyr | 0.03 | 0.1 | ND | Methyl Parathion | 0.02 | 0.1 | ND | ||
| Mevinphos | 0.03 | 0.08 | ND | Abamectin | 0.03 | 0.08 | ND | ||
| Acephate | 0.02 | 0.05 | ND | Acetamiprid | 0.01 | 0.05 | ND | ||
| Azoxystrobin | 0.01 | 0.02 | ND | Bifenazate | 0.01 | 0.05 | ND | ||
| Bifenthrin | 0.02 | 0.35 | ND | Boscalid | 0.01 | 0.03 | ND | ||
| Carbaryl | 0.01 | 0.02 | ND | Chlorantraniliprole | 0.01 | 0.04 | ND | ||
| Clofentezine | 0.01 | 0.03 | ND | Diazinon | 0.01 | 0.02 | ND | ||
| Dimethomorph | 0.02 | 0.06 | ND | Etoxazole | 0.01 | 0.05 | ND | ||
| Fenpyroximate | 0.02 | 0.1 | ND | Flonicamid | 0.01 | 0.02 | ND | ||
| Fludioxonil | 0.01 | 0.05 | ND | Hexythiazox | 0.01 | 0.03 | ND | ||
| Imidacloprid | 0.01 | 0.05 | ND | Kresoxim-methyl | 0.01 | 0.03 | ND | ||
| Malathion | 0.01 | 0.05 | ND | Metalaxyl | 0.01 | 0.02 | ND | ||
| Methomyl | 0.02 | 0.05 | ND | Myclobutanil | 0.02 | 0.07 | ND | ||
| Naled | 0.01 | 0.02 | ND | Oxamyl | 0.01 | 0.02 | ND | ||
| Permethrin | 0.01 | 0.02 | ND | Phosmet | 0.01 | 0.02 | ND | ||
| Piperonyl Butoxide | 0.02 | 0.06 | ND | Propiconazole | 0.03 | 0.08 | ND | ||
| Prallethrin | 0.02 | 0.05 | ND | Pyrethrin | 0.05 | 0.41 | ND | ||
| Pyridaben | 0.02 | 0.07 | ND | Spinosad A | 0.01 | 0.05 | ND | ||
| Spinosad D | 0.01 | 0.05 | ND | Spiromesifen | 0.02 | 0.06 | ND | ||
| Spirotetramat | 0.01 | 0.02 | ND | Tebuconazole | 0.01 | 0.02 | ND | ||
| Thiamethoxam | 0.01 | 0.02 | ND | Trifloxystrobin | 0.01 | 0.02 | ND | ||
| Acequinocyl | 0.02 | 0.09 | ND | Captan | 0.01 | 0.02 | ND | ||
| Cypermethrin | 0.02 | 0.1 | ND | Cyfluthrin | 0.04 | 0.1 | ND | ||
| Fenhexamid | 0.02 | 0.07 | ND | Spinetoram J,L | 0.02 | 0.07 | ND | ||
| Pentachloronitrobenzene | 0.01 | 0.1 | ND | Chlormequat Chloride | 0.02 | 0.1 | NT |
RES - Residual Solvents
Analyzed Aug 31, 2022 | Instrument GC/FID with Headspace Analyzer | Method SOP-006| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Propane (Prop) | 0.044 | 0.4 | ND | 5000 | Butane (But) | 0.02 | 0.4 | ND | 5000 |
| Methanol (Metha) | 1.176 | 3.92 | ND | 3000 | Ethylene Oxide (EthOx) | 0.08 | 0.4 | ND | 1 |
| Pentane (Pen) | 0.024 | 0.4 | ND | 5000 | Ethanol (Ethan) | 0.048 | 0.4 | ND | 5000 |
| Ethyl Ether (EthEt) | 0.036 | 0.4 | ND | 5000 | Acetone (Acet) | 0.044 | 0.4 | ND | 5000 |
| Isopropanol (2-Pro) | 1.16 | 3.868 | ND | 5000 | Acetonitrile (Acetonit) | 0.888 | 2.952 | ND | 410 |
| Methylene Chloride (MetCh) | 0.04 | 0.4 | ND | 1 | Hexane (Hex) | 0.012 | 0.4 | ND | 290 |
| Ethyl Acetate (EthAc) | 0.032 | 0.4 | ND | 5000 | Chloroform (Clo) | 0.028 | 0.4 | ND | 1 |
| Benzene (Ben) | 0.012 | 0.4 | ND | 1 | 1-2-Dichloroethane (12-Dich) | 0.024 | 0.4 | ND | 1 |
| Heptane (Hep) | 0.012 | 0.4 | ND | 5000 | Trichloroethylene (TriClEth) | 0.072 | 0.4 | ND | 1 |
| Toluene | 0.036 | 0.4 | ND | 890 | Xylenes (Xyl) | 0.012 | 0.4 | ND | 2170 |
FVI - Filth & Foreign Material Inspection
Analyzed Aug 29, 2022 | Instrument Microscope | Method SOP-010| Analyte / Limit | Result |
Analyte / Limit | Result |
|---|---|---|---|
|
> 1/4 of the total sample area covered by sand, soil, cinders, or dirt |
ND |
> 1/4 of the total sample area covered by mold |
ND |
|
> 1 insect fragment, 1 hair, or 1 count mammalian excreta per 3g |
ND |
> 1/4 of the total sample area covered by an imbedded foreign material |
ND |