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PharmLabs San Diego Certificate of Analysis
Sample Tropical 13mg D9/87mg D8
Delta9 THC 2.21% THCa ND Total THC (THC + THCa) 2.21% Delta8 THC 20.76%
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Sample ID  SD221028-003 (54172) Matrix   Edible (Other Cannabis Good)
Tested for  Pacific Manufacturing and Design
Sampled   - Received   Oct 27, 2022 Reported   Nov 11, 2022
Analyses executed   FP-NI20 Unit Mass (g)   4.5 Serving Size (g)   4.5

CANX - Cannabinoids

Analyzed Nov 10, 2022  |  Instrument HPLC-VWD  | Method SOP-001
The expanded Uncertainty of the Cannabinoid analysis is approximately ±7.806% at the 95% Confidence Level
Analyte   LOD
mg/g
LOQ
mg/g
Result
%
Result
mg/g
Result
mg/Serving
Result
mg/Unit
Sample photography
11-Hydroxy-Δ8-Tetrahydrocannabivarin (11-Hyd-Δ8-THCV)   0.013 0.041 ND ND ND ND Photo-2022-11-08-17-18-38
Cannabidiorcin (CBDO)   0.002 0.007 ND ND ND ND
Abnormal Cannabidiorcin (a-CBDO)   0.01 0.031 ND ND ND ND
(+/-)-9B-hydroxy-Hexahydrocannibinol (9b-HHC)   0.012 0.036 ND ND ND ND
11-Hydroxy-Δ8-Tetrahydrocannabinol (11-Hyd-Δ8-THC)   0.007 0.021 ND ND ND ND
Cannabidiolic Acid (CBDA)   0.001 0.16 ND ND ND ND
Cannabigerol Acid (CBGA)   0.001 0.16 ND ND ND ND
Cannabigerol (CBG)   0.001 0.16 0.00 0.03 0.12 0.12
Cannabidiol (CBD)   0.001 0.16 0.01 0.09 0.40 0.40
1(S)-THD (s-THD)   0.013 0.041 ND ND ND ND
1(R)-THD (r-THD)   0.025 0.075 ND ND ND ND
Tetrahydrocannabivarin (THCV)   0.001 0.16 ND ND ND ND
Δ8-tetrahydrocannabivarin (Δ8-THCV)   0.021 0.064 ND ND ND ND
Tetrahydrocannabutol (Δ9-THCB)   0.013 0.038 ND ND ND ND
Cannabinol (CBN)   0.001 0.16 0.00 0.03 0.15 0.15
exo-THC (exo-THC)   0.005 0.16 ND ND ND ND
Tetrahydrocannabinol (Δ9-THC)   0.003 0.16 0.22 2.21 9.95 9.95
Δ8-tetrahydrocannabinol (Δ8-THC)   0.004 0.16 2.08 20.76 93.41 93.41
(6aR,9S)-Δ10-Tetrahydrocannabinol ((6aR,9S)-Δ10)   0.015 0.16 ND ND ND ND
Hexahydrocannabinol (S Isomer) (9s-HHC)   0.017 0.16 ND ND ND ND
(6aR,9R)-Δ10-Tetrahydrocannabinol ((6aR,9R)-Δ10)   0.007 0.16 ND ND ND ND
Hexahydrocannabinol (R Isomer) (9r-HHC)   0.016 0.16 ND ND ND ND
Tetrahydrocannabinolic Acid (THCA)   0.001 0.16 ND ND ND ND
Δ9-Tetrahydrocannabihexol (Δ9-THCH)   0.024 0.071 ND ND ND ND
Cannabinol Acetate (CBNO)   0.014 0.043 ND ND ND ND
Δ9-Tetrahydrocannabiphorol (Δ9-THCP)   0.017 0.16 ND ND ND ND
Δ8-Tetrahydrocannabiphorol (Δ8-THCP)   0.041 0.16 ND ND ND ND
Δ8-THC-O-acetate (Δ8-THCO)   0.076 0.16 ND ND ND ND
9(S)-HHCP (s-HHCP)   0.031 0.094 ND ND ND ND
Δ9-THC-O-acetate (Δ9-THCO)   0.066 0.16 ND ND ND ND
9(R)-HHCP (r-HHCP)   0.026 0.079 ND ND ND ND
3-octyl-Δ8-Tetrahydrocannabinol (Δ8-THC-C8)   0.067 0.204 ND ND ND ND
Total THC ( THCa * 0.877 + Δ9THC )       0.22 2.21 9.95 9.95
Total THC + Δ8THC + Δ10THC ( THCa * 0.877 + Δ9THC + Δ8THC + Δ10THC )       2.30 22.97 103.36 103.36
Total CBD ( CBDa * 0.877 + CBD )       0.01 0.09 0.40 0.40
Total CBG ( CBGa * 0.877 + CBG )       0.00 0.03 0.12 0.12
Total HHC ( 9r-HHC + 9s-HHC )       ND ND ND ND
Total Cannabinoids Analyzed       2.31 23.12 104.03 104.03

HME - Heavy Metals

Analyzed Nov 11, 2022  |  Instrument ICP/MSMS  | Method SOP-005
Analyte LOD
ug/g
LOQ
ug/g
Result
ug/g
Limit
ug/g
Arsenic (As) 0.0009 0.0027 <LOQ 1.5
Cadmium (Cd) 0.0005 0.0015 <LOQ 0.5
Mercury (Hg) 0.0058 0.0174 ND 3
Lead (Pb) 0.0006 0.0018 <LOQ 0.5
Nickel (Ni) 6.0e-05 0.0002 NT

MIBNIG - Microbial

Analyzed Nov 10, 2022  |  Instrument Plating  | Method SOP-007
Analyte LOD
LOQ
Result
CFU/g
Limit Analyte LOD
LOQ
Result
CFU/g
Limit
Shiga toxin-producing Escherichia Coli ND ND per 1 gram Salmonella spp. ND ND per 1 gram

MTO - Mycotoxin

Analyzed Nov 11, 2022  |  Instrument LC/MSMS  | Method SOP-004
Analyte LOD
ug/kg
LOQ
ug/kg
Result
ug/kg (ppb)
Limit
ug/kg
Analyte LOD
ug/kg
LOQ
ug/kg
Result
ug/kg (ppb)
Limit
ug/kg
Ochratoxin A 5.0 20.0 ND 20 Aflatoxin B1 2.5 5.0 ND -
Aflatoxin B2 2.5 5.0 ND - Aflatoxin G1 2.5 5.0 ND -
Aflatoxin G2 2.5 5.0 ND - Total Aflatoxins 10.0 20.0 ND 20

PES - Pesticides

Analyzed Nov 11, 2022  |  Instrument LC/MSMS GC/MSMS  | Method SOP-003
Analyte LOD
ug/g
LOQ
ug/g
Result
ug/g
Limit
ug/g
Analyte LOD
ug/g
LOQ
ug/g
Result
ug/g
Limit
ug/g
Aldicarb 0.0078 0.02 ND 0.0078 Carbofuran 0.01 0.02 ND 0.01
Dimethoate 0.01 0.02 ND 0.01 Etofenprox 0.02 0.1 ND 0.02
Fenoxycarb 0.01 0.02 ND 0.01 Thiachloprid 0.01 0.02 ND 0.01
Daminozide 0.01 0.03 ND 0.01 Dichlorvos 0.02 0.07 ND 0.02
Imazalil 0.02 0.07 ND 0.02 Methiocarb 0.01 0.02 ND 0.01
Spiroxamine 0.01 0.02 ND 0.01 Coumaphos 0.01 0.02 ND 0.01
Fipronil 0.01 0.1 ND 0.01 Paclobutrazol 0.01 0.03 ND 0.01
Chlorpyrifos 0.01 0.04 ND 0.01 Ethoprophos (Prophos) 0.01 0.02 ND 0.01
Baygon (Propoxur) 0.01 0.02 ND 0.01 Chlordane 0.04 0.1 ND 0.04
Chlorfenapyr 0.03 0.1 ND 0.03 Methyl Parathion 0.02 0.1 ND 0.02
Mevinphos 0.03 0.08 ND 0.03 Abamectin 0.03 0.08 ND 0.3
Acephate 0.02 0.05 ND 5 Acetamiprid 0.01 0.05 ND 5
Azoxystrobin 0.01 0.02 ND 40 Bifenazate 0.01 0.05 ND 5
Bifenthrin 0.02 0.35 ND 0.5 Boscalid 0.01 0.03 ND 10
Carbaryl 0.01 0.02 ND 0.5 Chlorantraniliprole 0.01 0.04 ND 40
Clofentezine 0.01 0.03 ND 0.5 Diazinon 0.01 0.02 ND 0.2
Dimethomorph 0.02 0.06 ND 20 Etoxazole 0.01 0.05 ND 1.5
Fenpyroximate 0.02 0.1 ND 2 Flonicamid 0.01 0.02 ND 2
Fludioxonil 0.01 0.05 ND 30 Hexythiazox 0.01 0.03 ND 2
Imidacloprid 0.01 0.05 ND 3 Kresoxim-methyl 0.01 0.03 ND 1
Malathion 0.01 0.05 ND 5 Metalaxyl 0.01 0.02 ND 15
Methomyl 0.02 0.05 ND 0.1 Myclobutanil 0.02 0.07 ND 9
Naled 0.01 0.02 ND 0.5 Oxamyl 0.01 0.02 ND 0.2
Permethrin 0.01 0.02 ND 20 Phosmet 0.01 0.02 ND 0.2
Piperonyl Butoxide 0.02 0.06 ND 8 Propiconazole 0.03 0.08 ND 20
Prallethrin 0.02 0.05 ND 0.4 Pyrethrin 0.05 0.41 ND 1
Pyridaben 0.02 0.07 ND 3 Spinosad A 0.01 0.05 ND 3
Spinosad D 0.01 0.05 ND 3 Spiromesifen 0.02 0.06 ND 12
Spirotetramat 0.01 0.02 ND 13 Tebuconazole 0.01 0.02 ND 2
Thiamethoxam 0.01 0.02 ND 4.5 Trifloxystrobin 0.01 0.02 ND 30
Acequinocyl 0.02 0.09 ND 4 Captan 0.01 0.02 ND 5
Cypermethrin 0.02 0.1 ND 1 Cyfluthrin 0.04 0.1 ND 1
Fenhexamid 0.02 0.07 ND 10 Spinetoram J,L 0.02 0.07 ND 3
Pentachloronitrobenzene 0.01 0.1 ND 0.2  

RES - Residual Solvents

Analyzed Nov 11, 2022  |  Instrument GC/FID with Headspace Analyzer  | Method SOP-006
Analyte LOD
ug/g
LOQ
ug/g
Result
ug/g
Limit
ug/g
Analyte LOD
ug/g
LOQ
ug/g
Result
ug/g
Limit
ug/g
Propane (Prop) 0.4 40.0 ND 5000 Butane (But) 0.4 40.0 ND 5000
Methanol (Metha) 0.4 40.0 ND 3000 Ethylene Oxide (EthOx) 0.4 0.8 ND 1
Pentane (Pen) 0.4 40.0 ND 5000 Ethanol (Ethan) 0.4 40.0 ND 5000
Ethyl Ether (EthEt) 0.4 40.0 ND 5000 Acetone (Acet) 0.4 40.0 ND 5000
Isopropanol (2-Pro) 0.4 40.0 ND 5000 Acetonitrile (Acetonit) 0.4 40.0 ND 410
Methylene Chloride (MetCh) 0.4 0.8 ND 1 Hexane (Hex) 0.4 40.0 ND 290
Ethyl Acetate (EthAc) 0.4 40.0 ND 5000 Chloroform (Clo) 0.4 0.8 ND 1
Benzene (Ben) 0.4 0.8 ND 1 1-2-Dichloroethane (12-Dich) 0.4 0.8 ND 1
Heptane (Hep) 0.4 40.0 ND 5000 Trichloroethylene (TriClEth) 0.4 0.8 ND 1
Toluene (Toluene) 0.4 40.0 ND 890 Xylenes (Xyl) 0.4 40.0 ND 2170

FVI - Filth & Foreign Material Inspection

Analyzed Nov 03, 2022  |  Instrument Microscope  | Method SOP-010
Analyte / Limit Result
Analyte / Limit Result
> 1/4 of the total sample area
covered by sand, soil, cinders, or dirt
ND > 1/4 of the total sample area
covered by mold
ND
> 1 insect fragment, 1 hair, or 1 count
mammalian excreta per 3g
ND > 1/4 of the total sample area
covered by an imbedded foreign material
ND

MWA - Moisture Content & Water Activity

Analyzed Nov 11, 2022  |  Instrument Chilled-mirror Dewpoint and Capacitance  | Method SOP-008
Analyte LOD
%
LOQ
%
Result
Limit Analyte LOD
%
LOQ
%
Result
Limit
Moisture (Moi) 0.0 0.0 3.8 % Mw 13 % Mw Water Activity (WA) 0.03 0.03 0.26 aw 0.85 aw