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PharmLabs San Diego
Certificate of Analysis
Sample
Delta 8 Distillate
Delta9 THC
UI
THCa
ND
Total THC (THC + THCa)
UI
Delta8 THC
99.10%
| Sample ID SD221123-005 (55716) | Matrix Concentrate (Inhalable Cannabis Good) | Batch ID/Lot ID D8DISTB167 |
| Tested for Aculliance Holdings |
| Sampled - | Received Nov 23, 2022 | Reported Dec 01, 2022 |
| Analyses executed CAN+, RES, MIBIG, MTO, PES, HME, FVI | |||||
Laboratory note: The estimated concentration of the unknown peak in the sample is 4.24% | Currently PharmLabs laboratory can not confirm an unidentified peak in your chromatogram due to interference (only with highly concentrated D8 products) from which we believe to be either (+)d8-THC or d9-THC. At this time there are no reference standards available for (+)d8-THC. (+)d8-THC is a different compound from the main (-)d8-THC cannabinoid and, therefore, these two compounds may have different efficacies. Using the most advanced instruments and techniques available, the separation of (+)d8-THC and d9-THC is problematic for the scientific community as a whole. PharmLabs believes the unidentified peak to be a combination of (+)d8-THC and d9-THC with the majority, if not all, of the concentration being (+)d8-THC. Total d8-THC is estimated to be 99.10%.
CAN+ - Cannabinoids
Analyzed Dec 01, 2022 | Instrument HPLC-VWD | Method SOP-001The expanded Uncertainty of the Cannabinoid analysis is approximately ±7.806% at the 95% Confidence Level
| Analyte |
LOD mg/g |
LOQ mg/g |
Result % |
Result mg/g |
|
|---|---|---|---|---|---|
| Cannabidivarin (CBDV) | 0.039 | 0.16 | ND | ND | |
| Cannabidiolic Acid (CBDA) | 0.001 | 0.16 | ND | ND | |
| Cannabigerol Acid (CBGA) | 0.001 | 0.16 | ND | ND | |
| Cannabigerol (CBG) | 0.001 | 0.16 | ND | ND | |
| Cannabidiol (CBD) | 0.001 | 0.16 | ND | ND | |
| Tetrahydrocannabivarin (THCV) | 0.001 | 0.16 | ND | ND | |
| Cannabinol (CBN) | 0.001 | 0.16 | <LOQ | <LOQ | |
| Tetrahydrocannabinol (Δ9-THC) | 0.003 | 0.16 | UI | UI | |
| Δ8-tetrahydrocannabinol (Δ8-THC) | 0.004 | 0.16 | 99.10 | 991.00 | |
| Cannabicyclol (CBL) | 0.002 | 0.16 | ND | ND | |
| Cannabichromene (CBC) | 0.002 | 0.16 | ND | ND | |
| Tetrahydrocannabinolic Acid (THCA) | 0.001 | 0.16 | ND | ND | |
| Total THC ( THCa * 0.877 + Δ9THC ) | UI | UI | |||
| Total THC + Δ8THC ( THCa * 0.877 + Δ9THC + Δ8THC ) | 99.10 | 991.00 | |||
| Total CBD ( CBDa * 0.877 + CBD ) | ND | ND | |||
| Total CBG ( CBGa * 0.877 + CBG ) | ND | ND | |||
| Total Cannabinoids Analyzed | 99.10 | 991.00 |
HME - Heavy Metals
Analyzed Nov 28, 2022 | Instrument ICP/MSMS | Method SOP-005| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|
| Arsenic (As) | 0.0009 | 0.0027 | <LOQ | 1.5 |
| Cadmium (Cd) | 0.0005 | 0.0015 | <LOQ | 0.5 |
| Mercury (Hg) | 0.0058 | 0.0174 | <LOQ | 3 |
| Lead (Pb) | 0.0006 | 0.0018 | 0.04 | 0.5 |
| Nickel (Ni) | 6.0e-05 | 0.0002 | NT |
MIBIG - Microbial
Analyzed Nov 28, 2022 | Instrument qPCR and/or Plating | Method SOP-007| Analyte |
LOD |
LOQ |
Result CFU/g |
Limit | Analyte |
LOD |
LOQ |
Result CFU/g |
Limit |
|---|---|---|---|---|---|---|---|---|---|
| Shiga toxin-producing Escherichia Coli | ND | ND per 1 gram | Salmonella spp. | ND | ND per 1 gram | ||||
| Aspergillus fumigatus | ND | ND per 1 gram | Aspergillus flavus | ND | ND per 1 gram | ||||
| Aspergillus niger | ND | ND per 1 gram | Aspergillus terreus | ND | ND per 1 gram |
MTO - Mycotoxin
Analyzed Nov 28, 2022 | Instrument LC/MSMS | Method SOP-004| Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg (ppb) |
Limit ug/kg |
Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg (ppb) |
Limit ug/kg |
|---|---|---|---|---|---|---|---|---|---|
| Ochratoxin A | 5.0 | 20.0 | ND | 20 | Aflatoxin B1 | 2.5 | 5.0 | ND | - |
| Aflatoxin B2 | 2.5 | 5.0 | ND | - | Aflatoxin G1 | 2.5 | 5.0 | ND | - |
| Aflatoxin G2 | 2.5 | 5.0 | ND | - | Total Aflatoxins | 10.0 | 20.0 | ND | 20 |
PES - Pesticides
Analyzed Nov 28, 2022 | Instrument LC/MSMS GC/MSMS | Method SOP-003| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Aldicarb | 0.0078 | 0.02 | ND | 0.0078 | Carbofuran | 0.01 | 0.02 | ND | 0.01 |
| Dimethoate | 0.01 | 0.02 | ND | 0.01 | Etofenprox | 0.02 | 0.1 | ND | 0.02 |
| Fenoxycarb | 0.01 | 0.02 | ND | 0.01 | Thiachloprid | 0.01 | 0.02 | ND | 0.01 |
| Daminozide | 0.01 | 0.03 | ND | 0.01 | Dichlorvos | 0.02 | 0.07 | ND | 0.02 |
| Imazalil | 0.02 | 0.07 | ND | 0.02 | Methiocarb | 0.01 | 0.02 | ND | 0.01 |
| Spiroxamine | 0.01 | 0.02 | ND | 0.01 | Coumaphos | 0.01 | 0.02 | ND | 0.01 |
| Fipronil | 0.01 | 0.1 | ND | 0.01 | Paclobutrazol | 0.01 | 0.03 | ND | 0.01 |
| Chlorpyrifos | 0.01 | 0.04 | ND | 0.01 | Ethoprophos (Prophos) | 0.01 | 0.02 | ND | 0.01 |
| Baygon (Propoxur) | 0.01 | 0.02 | ND | 0.01 | Chlordane | 0.04 | 0.1 | ND | 0.04 |
| Chlorfenapyr | 0.03 | 0.1 | ND | 0.03 | Methyl Parathion | 0.02 | 0.1 | ND | 0.02 |
| Mevinphos | 0.03 | 0.08 | ND | 0.03 | Abamectin | 0.03 | 0.08 | ND | 0.1 |
| Acephate | 0.02 | 0.05 | ND | 0.1 | Acetamiprid | 0.01 | 0.05 | ND | 0.1 |
| Azoxystrobin | 0.01 | 0.02 | ND | 0.1 | Bifenazate | 0.01 | 0.05 | ND | 0.1 |
| Bifenthrin | 0.02 | 0.35 | ND | 3 | Boscalid | 0.01 | 0.03 | ND | 0.1 |
| Carbaryl | 0.01 | 0.02 | ND | 0.5 | Chlorantraniliprole | 0.01 | 0.04 | ND | 10 |
| Clofentezine | 0.01 | 0.03 | ND | 0.1 | Diazinon | 0.01 | 0.02 | ND | 0.1 |
| Dimethomorph | 0.02 | 0.06 | ND | 2 | Etoxazole | 0.01 | 0.05 | ND | 0.1 |
| Fenpyroximate | 0.02 | 0.1 | ND | 0.1 | Flonicamid | 0.01 | 0.02 | ND | 0.1 |
| Fludioxonil | 0.01 | 0.05 | ND | 0.1 | Hexythiazox | 0.01 | 0.03 | ND | 0.1 |
| Imidacloprid | 0.01 | 0.05 | ND | 5 | Kresoxim-methyl | 0.01 | 0.03 | ND | 0.1 |
| Malathion | 0.01 | 0.05 | ND | 0.5 | Metalaxyl | 0.01 | 0.02 | ND | 2 |
| Methomyl | 0.02 | 0.05 | ND | 1 | Myclobutanil | 0.02 | 0.07 | ND | 0.1 |
| Naled | 0.01 | 0.02 | ND | 0.1 | Oxamyl | 0.01 | 0.02 | ND | 0.5 |
| Permethrin | 0.01 | 0.02 | ND | 0.5 | Phosmet | 0.01 | 0.02 | ND | 0.1 |
| Piperonyl Butoxide | 0.02 | 0.06 | ND | 3 | Propiconazole | 0.03 | 0.08 | ND | 0.1 |
| Prallethrin | 0.02 | 0.05 | ND | 0.1 | Pyrethrin | 0.05 | 0.41 | ND | 0.5 |
| Pyridaben | 0.02 | 0.07 | ND | 0.1 | Spinosad A | 0.01 | 0.05 | ND | 0.1 |
| Spinosad D | 0.01 | 0.05 | ND | 0.1 | Spiromesifen | 0.02 | 0.06 | ND | 0.1 |
| Spirotetramat | 0.01 | 0.02 | ND | 0.1 | Tebuconazole | 0.01 | 0.02 | ND | 0.1 |
| Thiamethoxam | 0.01 | 0.02 | ND | 5 | Trifloxystrobin | 0.01 | 0.02 | ND | 0.1 |
| Acequinocyl | 0.02 | 0.09 | ND | 0.1 | Captan | 0.01 | 0.02 | ND | 0.7 |
| Cypermethrin | 0.02 | 0.1 | ND | 1 | Cyfluthrin | 0.04 | 0.1 | ND | 2 |
| Fenhexamid | 0.02 | 0.07 | ND | 0.1 | Spinetoram J,L | 0.02 | 0.07 | ND | 0.1 |
| Pentachloronitrobenzene | 0.01 | 0.1 | ND | 0.1 | |||||
RES - Residual Solvents
Analyzed Dec 01, 2022 | Instrument GC/FID with Headspace Analyzer | Method SOP-006| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Propane (Prop) | 0.4 | 40.0 | ND | 5000 | Butane (But) | 0.4 | 40.0 | ND | 5000 |
| Methanol (Metha) | 0.4 | 40.0 | ND | 3000 | Ethylene Oxide (EthOx) | 0.4 | 0.8 | <LOQ | 1 |
| Pentane (Pen) | 0.4 | 40.0 | ND | 5000 | Ethanol (Ethan) | 0.4 | 40.0 | ND | 5000 |
| Ethyl Ether (EthEt) | 0.4 | 40.0 | ND | 5000 | Acetone (Acet) | 0.4 | 40.0 | ND | 5000 |
| Isopropanol (2-Pro) | 0.4 | 40.0 | ND | 5000 | Acetonitrile (Acetonit) | 0.4 | 40.0 | ND | 410 |
| Methylene Chloride (MetCh) | 0.4 | 0.8 | <LOQ | 1 | Hexane (Hex) | 0.4 | 40.0 | ND | 290 |
| Ethyl Acetate (EthAc) | 0.4 | 40.0 | ND | 5000 | Chloroform (Clo) | 0.4 | 0.8 | ND | 1 |
| Benzene (Ben) | 0.4 | 0.8 | ND | 1 | 1-2-Dichloroethane (12-Dich) | 0.4 | 0.8 | ND | 1 |
| Heptane (Hep) | 0.4 | 40.0 | ND | 5000 | Trichloroethylene (TriClEth) | 0.4 | 0.8 | ND | 1 |
| Toluene (Toluene) | 0.4 | 40.0 | ND | 890 | Xylenes (Xyl) | 0.4 | 40.0 | ND | 2170 |
FVI - Filth & Foreign Material Inspection
Analyzed Nov 23, 2022 | Instrument Microscope | Method SOP-010| Analyte / Limit | Result |
Analyte / Limit | Result |
|---|---|---|---|
|
> 1/4 of the total sample area covered by sand, soil, cinders, or dirt |
ND |
> 1/4 of the total sample area covered by mold |
ND |
|
> 1 insect fragment, 1 hair, or 1 count mammalian excreta per 3g |
ND |
> 1/4 of the total sample area covered by an imbedded foreign material |
ND |