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PharmLabs San Diego
Certificate of Analysis
Sample
Kruz Blueberry Kush 1G
Delta9 THC
UI
THCa
20.95%
Total THC (THCa * 0.877 + THC)
18.37%
Delta8 THC
11.64%
| Sample ID SD230725-067 (81648) | Matrix Flower |
| Tested for Kruz |
| Sampled - | Received Jul 25, 2023 | Reported Sep 01, 2023 |
| Analyses executed FP-IO20, QARUSH | |||||
Laboratory note: The estimated concentration of the unknown peak in the sample is 1.65% | Currently PharmLabs laboratory can not confirm an unidentified peak in your chromatogram due to interference (only with highly concentrated D8 products) from which we believe to be either (+)d8-THC or d9-THC. At this time there are no reference standards available for (+)d8-THC. (+)d8-THC is a different compound from the main (-)d8-THC cannabinoid and, therefore, these two compounds may have different efficacies. Using the most advanced instruments and techniques available, the separation of (+)d8-THC and d9-THC is problematic for the scientific community as a whole. PharmLabs believes the unidentified peak to be a combination of (+)d8-THC and d9-THC with the majority, if not all, of the concentration being (+)d8-THC. Total (+/-) D8 Concentration is estimated to be: 11.64%
CANx - Cannabinoids
Analyzed Aug 01, 2023 | Instrument HPLC-VWD | Method SOP-001The expanded Uncertainty of the Cannabinoids analysis is approximately ± 7.806% at the 95% Confidence Level
| Analyte |
LOD mg/g |
LOQ mg/g |
Result % |
Result mg/g |
|
|---|---|---|---|---|---|
| 11-Hydroxy-Δ8-Tetrahydrocannabivarin (11-Hyd-Δ8-THCV) | 0.013 | 0.041 | ND | ND | |
| Cannabidiorcin (CBDO) | 0.006 | 0.02 | ND | ND | |
| Abnormal Cannabidiorcin (a-CBDO) | 0.013 | 0.038 | ND | ND | |
| (+/-)-9B-hydroxy-Hexahydrocannibinol (9b-HHC) | 0.015 | 0.045 | ND | ND | |
| 11-Hydroxy-Δ8-Tetrahydrocannabinol (11-Hyd-Δ8-THC) | 0.015 | 0.045 | ND | ND | |
| Cannabidiolic Acid (CBDA) | 0.033 | 0.16 | 7.37 | 73.68 | |
| Cannabigerol Acid (CBGA) | 0.033 | 0.16 | 1.46 | 14.64 | |
| Cannabigerol (CBG) | 0.048 | 0.16 | 0.24 | 2.43 | |
| Cannabidiol (CBD) | 0.069 | 0.229 | 1.06 | 10.58 | |
| 1(S)-Tetrahydrocannabidiol (1(S)-H4-CBD) | 0.008 | 0.026 | ND | ND | |
| 1(R)-Tetrahydrocannabidiol (1(R)-H4-CBD) | 0.016 | 0.049 | ND | ND | |
| Tetrahydrocannabivarin (THCV) | 0.049 | 0.162 | ND | ND | |
| Δ8-tetrahydrocannabivarin (Δ8-THCV) | 0.012 | 0.036 | ND | ND | |
| Cannabidihexol (CBDH) | 0.005 | 0.16 | ND | ND | |
| Tetrahydrocannabutol (Δ9-THCB) | 0.01 | 0.029 | ND | ND | |
| Cannabinol (CBN) | 0.047 | 0.16 | 4.31 | 43.09 | |
| Cannabidiphorol (CBDP) | 0.016 | 0.049 | ND | ND | |
| exo-THC (exo-THC) | 0.016 | 0.8 | ND | ND | |
| Tetrahydrocannabinol (Δ9-THC) | 0.092 | 0.307 | UI | UI | |
| Δ8-tetrahydrocannabinol (Δ8-THC) | 0.044 | 0.16 | 11.64 | 116.40 | |
| (6aR,9S)-Δ10-Tetrahydrocannabinol ((6aR,9S)-Δ10) | 0.015 | 0.8 | ND | ND | |
| Hexahydrocannabinol (S Isomer) (9s-HHC) | 0.017 | 0.8 | 0.50 | 4.97 | |
| (6aR,9R)-Δ10-Tetrahydrocannabinol ((6aR,9R)-Δ10) | 0.007 | 0.8 | ND | ND | |
| Hexahydrocannabinol (R Isomer) (9r-HHC) | 0.016 | 0.8 | 0.74 | 7.40 | |
| Tetrahydrocannabinolic Acid (THCA) | 0.117 | 0.389 | 20.95 | 209.47 | |
| Δ9-Tetrahydrocannabihexol (Δ9-THCH) | 0.02 | 0.061 | ND | ND | |
| Cannabinol Acetate (CBNO) | 0.009 | 0.027 | ND | ND | |
| Δ9-Tetrahydrocannabiphorol (Δ9-THCP) | 0.017 | 0.8 | ND | ND | |
| Δ8-Tetrahydrocannabiphorol (Δ8-THCP) | 0.041 | 0.8 | ND | ND | |
| Cannabicitran (CBT) | 0.005 | 0.16 | ND | ND | |
| Δ8-THC-O-acetate (Δ8-THCO) | 0.076 | 0.8 | ND | ND | |
| 9(S)-HHCP (s-HHCP) | 0.013 | 0.041 | ND | ND | |
| Δ9-THC-O-acetate (Δ9-THCO) | 0.066 | 0.8 | ND | ND | |
| 9(R)-HHCP (r-HHCP) | 0.015 | 0.045 | ND | ND | |
| 9(S)-HHC-O-acetate (s-HHCO) | 0.005 | 0.16 | ND | ND | |
| 9(R)-HHC-O-acetate (r-HHCO) | 0.031 | 0.093 | ND | ND | |
| 3-octyl-Δ8-Tetrahydrocannabinol (Δ8-THC-C8) | 0.021 | 0.062 | ND | ND | |
| Total THC ( THCa * 0.877 + Δ9THC ) | 18.37 | 183.71 | |||
| Total THC + Δ8THC + Δ10THC ( THCa * 0.877 + Δ9THC + Δ8THC + Δ10THC ) | 30.01 | 300.11 | |||
| Total CBD ( CBDa * 0.877 + CBD ) | 7.52 | 75.19 | |||
| Total CBG ( CBGa * 0.877 + CBG ) | 1.53 | 15.27 | |||
| Total HHC ( 9r-HHC + 9s-HHC ) | 1.24 | 12.37 | |||
| Total Cannabinoids Analyzed | 44.60 | 446.03 |
*Dry Weight %
HME - Heavy Metals
Analyzed Jul 28, 2023 | Instrument ICP/MSMS | Method SOP-005| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|
| Arsenic (As) | 0.0009 | 0.0027 | 0.17 | 1.5 |
| Cadmium (Cd) | 0.0005 | 0.0015 | 0.08 | 0.5 |
| Mercury (Hg) | 0.0058 | 0.0174 | 0.00 | 3 |
| Lead (Pb) | 0.0006 | 0.0018 | 0.12 | 0.5 |
MIBIG - Microbial
Analyzed Jul 27, 2023 | Instrument qPCR and/or Plating | Method SOP-007| Analyte |
LOD CFU/g |
LOQ CFU/g |
Result CFU/g |
Limit CFU/g |
|---|---|---|---|---|
| Shiga toxin-producing Escherichia Coli | 1.0 | 1.0 | Negative | 1 |
| Salmonella spp. | 1.0 | 1.0 | Negative | 1 |
| Aspergillus fumigatus | 1.0 | 1.0 | Negative | 1 |
| Aspergillus flavus | 1.0 | 1.0 | Negative | 1 |
| Aspergillus niger | 1.0 | 1.0 | ND | 1 |
| Aspergillus terreus | 1.0 | 1.0 | Negative | 1 |
MTO - Mycotoxin
Analyzed Jul 31, 2023 | Instrument LC/MSMS | Method SOP-004| Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
|---|---|---|---|---|---|---|---|---|---|
| Ochratoxin A | 5.0 | 20.0 | ND | 20 | Aflatoxin B1 | 2.5 | 5.0 | ND | - |
| Aflatoxin B2 | 2.5 | 5.0 | ND | - | Aflatoxin G1 | 2.5 | 5.0 | ND | - |
| Aflatoxin G2 | 2.5 | 5.0 | ND | - | Total Aflatoxins | 10.0 | 20.0 | ND | 20 |
PES - Pesticides
Analyzed Aug 30, 2023 | Instrument LC/MSMS GC/MSMS | Method SOP-003| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Aldicarb | 0.01 | 0.02 | ND | Carbofuran | 0.01 | 0.02 | ND | ||
| Dimethoate | 0.01 | 0.02 | ND | Etofenprox | 0.02 | 0.1 | ND | ||
| Fenoxycarb | 0.01 | 0.02 | ND | Thiachloprid | 0.01 | 0.02 | ND | ||
| Daminozide | 0.01 | 0.03 | ND | Dichlorvos | 0.02 | 0.07 | ND | ||
| Imazalil | 0.02 | 0.07 | ND | Methiocarb | 0.01 | 0.02 | ND | ||
| Spiroxamine | 0.01 | 0.02 | ND | Coumaphos | 0.01 | 0.02 | ND | ||
| Fipronil | 0.01 | 0.1 | ND | Paclobutrazol | 0.01 | 0.03 | ND | ||
| Chlorpyrifos | 0.01 | 0.04 | ND | Ethoprophos (Prophos) | 0.01 | 0.02 | ND | ||
| Baygon (Propoxur) | 0.01 | 0.02 | ND | Chlordane | 0.04 | 0.1 | ND | ||
| Chlorfenapyr | 0.03 | 0.1 | <LOQ | Methyl Parathion | 0.02 | 0.1 | ND | ||
| Mevinphos | 0.03 | 0.08 | ND | Abamectin | 0.03 | 0.08 | ND | ||
| Acephate | 0.02 | 0.05 | ND | Acetamiprid | 0.01 | 0.05 | ND | ||
| Azoxystrobin | 0.01 | 0.02 | ND | Bifenazate | 0.01 | 0.05 | ND | ||
| Bifenthrin | 0.02 | 0.35 | ND | Boscalid | 0.01 | 0.03 | ND | ||
| Carbaryl | 0.01 | 0.02 | ND | Chlorantraniliprole | 0.01 | 0.04 | ND | ||
| Clofentezine | 0.01 | 0.03 | ND | Diazinon | 0.01 | 0.02 | ND | ||
| Dimethomorph | 0.02 | 0.06 | ND | Etoxazole | 0.01 | 0.05 | ND | ||
| Fenpyroximate | 0.02 | 0.1 | ND | Flonicamid | 0.01 | 0.02 | ND | ||
| Fludioxonil | 0.01 | 0.05 | ND | Hexythiazox | 0.01 | 0.03 | ND | ||
| Imidacloprid | 0.01 | 0.05 | ND | Kresoxim-methyl | 0.01 | 0.03 | ND | ||
| Malathion | 0.01 | 0.05 | ND | Metalaxyl | 0.01 | 0.02 | ND | ||
| Methomyl | 0.02 | 0.05 | ND | Myclobutanil | 0.02 | 0.07 | ND | ||
| Naled | 0.01 | 0.02 | ND | Oxamyl | 0.01 | 0.02 | ND | ||
| Permethrin | 0.01 | 0.02 | ND | Phosmet | 0.01 | 0.02 | ND | ||
| Piperonyl Butoxide | 0.02 | 0.06 | ND | Propiconazole | 0.03 | 0.08 | ND | ||
| Prallethrin | 0.02 | 0.05 | ND | Pyrethrin | 0.05 | 0.41 | ND | ||
| Pyridaben | 0.02 | 0.07 | ND | Spinosad A | 0.01 | 0.05 | ND | ||
| Spinosad D | 0.01 | 0.05 | ND | Spiromesifen | 0.02 | 0.06 | ND | ||
| Spirotetramat | 0.01 | 0.02 | ND | Tebuconazole | 0.01 | 0.02 | ND | ||
| Thiamethoxam | 0.01 | 0.02 | ND | Trifloxystrobin | 0.01 | 0.02 | ND | ||
| Acequinocyl | 0.02 | 0.09 | ND | Captan | 0.01 | 0.02 | ND | ||
| Cypermethrin | 0.02 | 0.1 | ND | Cyfluthrin | 0.04 | 0.1 | ND | ||
| Fenhexamid | 0.02 | 0.07 | ND | Spinetoram J,L | 0.02 | 0.07 | ND | ||
| Pentachloronitrobenzene | 0.01 | 0.1 | ND | Chlormequat Chloride | 0.02 | 0.1 | NT |
RES - Residual Solvents
Analyzed Sep 01, 2023 | Instrument GC/FID with Headspace Analyzer | Method SOP-006| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Propane (Prop) | 0.044 | 0.4 | ND | Butane (But) | 0.02 | 0.4 | ND | ||
| Methanol (Metha) | 1.176 | 3.92 | ND | Ethylene Oxide (EthOx) | 0.08 | 0.4 | ND | ||
| Pentane (Pen) | 0.024 | 0.4 | ND | Ethanol (Ethan) | 0.048 | 0.4 | ND | ||
| Ethyl Ether (EthEt) | 0.036 | 0.4 | ND | Acetone (Acet) | 0.044 | 0.4 | 52.9 | ||
| Isopropanol (2-Pro) | 1.16 | 3.868 | ND | Acetonitrile (Acetonit) | 0.888 | 2.952 | ND | ||
| Methylene Chloride (MetCh) | 0.04 | 0.4 | ND | Hexane (Hex) | 0.012 | 0.4 | ND | ||
| Ethyl Acetate (EthAc) | 0.032 | 0.4 | ND | Chloroform (Clo) | 0.028 | 0.4 | 54.8 | ||
| Benzene (Ben) | 0.012 | 0.4 | ND | 1-2-Dichloroethane (12-Dich) | 0.024 | 0.4 | ND | ||
| Heptane (Hep) | 0.012 | 0.4 | <LOQ | Trichloroethylene (TriClEth) | 0.072 | 0.4 | ND | ||
| Toluene | 0.036 | 0.4 | ND | Xylenes (Xyl) | 0.012 | 0.4 | ND |
FVI - Filth & Foreign Material Inspection
Analyzed Jul 26, 2023 | Instrument Microscope | Method SOP-010| Analyte / Limit | Result |
Analyte / Limit | Result |
|---|---|---|---|
|
> 1/4 of the total sample area covered by sand, soil, cinders, or dirt |
ND |
> 1/4 of the total sample area covered by mold |
ND |
|
> 1 insect fragment, 1 hair, or 1 count mammalian excreta per 3g |
ND |
> 1/4 of the total sample area covered by an imbedded foreign material |
ND |
MWA - Moisture Content & Water Activity
Analyzed Jul 26, 2023 | Instrument Chilled-mirror Dewpoint and Capacitance | Method SOP-008| Analyte |
LOD % |
LOQ % |
Result |
Limit | Analyte |
LOD % |
LOQ % |
Result |
Limit |
|---|---|---|---|---|---|---|---|---|---|
| Moisture (Moi) | 0.0 | 0.0 | 6.4 % Mw | 13 % Mw | Water Activity (WA) | 0.03 | 0.03 | 0.46 aw | 0.85 aw |