California / inhalable_product
kratom,metal,microbial,mycotoxin,pesticide,residual
download/print PDF version
reload with photo
PharmLabs San Diego
Certificate of Analysis
Sample
KTM Tablets - Zohm20240924-2
| Sample ID SD240926-102 (99839) | Matrix Concentrate |
| Tested for Zohm |
| Sampled - | Received Sep 25, 2024 | Reported Oct 21, 2024 |
| Analyses executed RES, MIBNIG, MTO, PES, HME, KTM | Unit Mass (g) 3.909 | Num. of Servings 5 | Serving Size (g) 0.78 | ||
Laboratory note: COA Update: 10/21/24 “Tested For” corrected as per client request
KTM - Kratom
Analyzed Sep 27, 2024 | Instrument HPLC VWD | Method SOP-KTMThe expanded Uncertainty of the Kratom analysis is approximately ± 7.81% at the 95% Confidence Level
| Analyte |
LOD ppm |
LOQ ppm |
Result % |
Result mg/g |
Result mg/Serving |
Result mg/Unit |
|---|---|---|---|---|---|---|
| 7-hydroxy Mitragynine (7HMG) | 0.008 | 0.025 | 2.15 | 21.49 | 16.76 | 84.00 |
| Mitragynine (MITG) | 0.018 | 0.054 | 0.02 | 0.21 | 0.16 | 0.82 |
| Speciogynine (SPEG) | 0.007 | 0.02 | ND | ND | ND | ND |
| Speciociliatine (SPCL) | 0.004 | 0.011 | ND | ND | ND | ND |
| Mitragynine Pseudoindoxyl (MITp) | 0.235 | 0.713 | NT | NT | NT | NT |
HME - Heavy Metals
Analyzed Sep 30, 2024 | Instrument ICP/MSMS | Method SOP-005| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|
| Arsenic (As) | 0.0009 | 0.0027 | ND | 1.5 |
| Cadmium (Cd) | 0.0005 | 0.0015 | ND | 0.5 |
| Mercury (Hg) | 0.0058 | 0.0174 | ND | 3 |
| Lead (Pb) | 0.0006 | 0.0018 | 0.01 | 0.5 |
| Nickel (Ni) | 6.0e-05 | 0.0002 | NT |
MIBNIG - Microbial
Analyzed Sep 30, 2024 | Instrument Plating | Method SOP-007| Analyte |
LOD CFU/g |
LOQ CFU/g |
Result CFU/g |
Limit CFU/g |
|---|---|---|---|---|
| Shiga toxin-producing Escherichia Coli | 1.0 | 1.0 | ND | |
| Salmonella spp. | 1.0 | 1.0 | ND |
MTO - Mycotoxin
Analyzed Oct 02, 2024 | Instrument LC/MSMS | Method SOP-004| Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
Analyte |
LOD ug/kg |
LOQ ug/kg |
Result ug/kg |
Limit ug/kg |
|---|---|---|---|---|---|---|---|---|---|
| Ochratoxin A | 5.0 | 20.0 | ND | 20 | Aflatoxin B1 | 2.5 | 5.0 | ND | - |
| Aflatoxin B2 | 2.5 | 5.0 | ND | - | Aflatoxin G1 | 2.5 | 5.0 | ND | - |
| Aflatoxin G2 | 2.5 | 5.0 | ND | - | Total Aflatoxins | 10.0 | 20.0 | ND | 20 |
PES - Pesticides
Analyzed Oct 02, 2024 | Instrument LC/MSMS GC/MSMS | Method SOP-003| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Aldicarb | 0.01 | 0.02 | ND | Carbofuran | 0.01 | 0.02 | ND | ||
| Dimethoate | 0.01 | 0.02 | ND | Etofenprox | 0.02 | 0.1 | ND | ||
| Fenoxycarb | 0.01 | 0.02 | ND | Thiachloprid | 0.01 | 0.02 | ND | ||
| Daminozide | 0.01 | 0.03 | ND | Dichlorvos | 0.02 | 0.07 | ND | ||
| Imazalil | 0.02 | 0.07 | ND | Methiocarb | 0.01 | 0.02 | ND | ||
| Spiroxamine | 0.01 | 0.02 | ND | Coumaphos | 0.01 | 0.02 | ND | ||
| Fipronil | 0.01 | 0.1 | NT | Paclobutrazol | 0.01 | 0.03 | ND | ||
| Chlorpyrifos | 0.01 | 0.04 | ND | Ethoprophos (Prophos) | 0.01 | 0.02 | ND | ||
| Baygon (Propoxur) | 0.01 | 0.02 | ND | Chlordane | 0.04 | 0.1 | NT | ||
| Chlorfenapyr | 0.03 | 0.1 | NT | Methyl Parathion | 0.02 | 0.1 | NT | ||
| Mevinphos | 0.03 | 0.08 | ND | Abamectin | 0.03 | 0.08 | ND | ||
| Acephate | 0.02 | 0.05 | ND | Acetamiprid | 0.01 | 0.05 | ND | ||
| Azoxystrobin | 0.01 | 0.02 | ND | Bifenazate | 0.01 | 0.05 | ND | ||
| Bifenthrin | 0.02 | 0.35 | ND | Boscalid | 0.01 | 0.03 | ND | ||
| Carbaryl | 0.01 | 0.02 | ND | Chlorantraniliprole | 0.01 | 0.04 | ND | ||
| Clofentezine | 0.01 | 0.03 | ND | Diazinon | 0.01 | 0.02 | ND | ||
| Dimethomorph | 0.02 | 0.06 | ND | Etoxazole | 0.01 | 0.05 | ND | ||
| Fenpyroximate | 0.02 | 0.1 | ND | Flonicamid | 0.01 | 0.02 | ND | ||
| Fludioxonil | 0.01 | 0.05 | ND | Hexythiazox | 0.01 | 0.03 | ND | ||
| Imidacloprid | 0.01 | 0.05 | ND | Kresoxim-methyl | 0.01 | 0.03 | ND | ||
| Malathion | 0.01 | 0.05 | ND | Metalaxyl | 0.01 | 0.02 | ND | ||
| Methomyl | 0.02 | 0.05 | ND | Myclobutanil | 0.02 | 0.07 | ND | ||
| Naled | 0.01 | 0.02 | ND | Oxamyl | 0.01 | 0.02 | ND | ||
| Permethrin | 0.01 | 0.02 | ND | Phosmet | 0.01 | 0.02 | ND | ||
| Piperonyl Butoxide | 0.02 | 0.06 | ND | Propiconazole | 0.03 | 0.08 | ND | ||
| Prallethrin | 0.02 | 0.05 | ND | Pyrethrin | 0.05 | 0.41 | ND | ||
| Pyridaben | 0.02 | 0.07 | ND | Spinosad A | 0.01 | 0.05 | ND | ||
| Spinosad D | 0.01 | 0.05 | ND | Spiromesifen | 0.02 | 0.06 | ND | ||
| Spirotetramat | 0.01 | 0.02 | ND | Tebuconazole | 0.01 | 0.02 | ND | ||
| Thiamethoxam | 0.01 | 0.02 | ND | Trifloxystrobin | 0.01 | 0.02 | ND | ||
| Acequinocyl | 0.02 | 0.09 | ND | Captan | 0.01 | 0.02 | ND | ||
| Cypermethrin | 0.02 | 0.1 | NT | Cyfluthrin | 0.04 | 0.1 | NT | ||
| Fenhexamid | 0.02 | 0.07 | ND | Spinetoram J,L | 0.02 | 0.07 | ND | ||
| Pentachloronitrobenzene | 0.01 | 0.1 | NT | Chlormequat Chloride | 0.02 | 0.1 | NT |
RES - Residual Solvents
Analyzed Sep 30, 2024 | Instrument GC/FID with Headspace Analyzer | Method SOP-006| Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
Analyte |
LOD ug/g |
LOQ ug/g |
Result ug/g |
Limit ug/g |
|---|---|---|---|---|---|---|---|---|---|
| Propane (Prop) | 0.044 | 0.4 | ND | 5000 | Butane (But) | 0.02 | 0.4 | ND | 5000 |
| Methanol (Metha) | 1.176 | 3.92 | 3743.2 | 3000 | Ethylene Oxide (EthOx) | 0.08 | 0.4 | ND | 1 |
| Pentane (Pen) | 0.024 | 0.4 | ND | 5000 | Ethanol (Ethan) | 0.048 | 0.4 | <LOQ | 5000 |
| Ethyl Ether (EthEt) | 0.036 | 0.4 | ND | 5000 | Acetone (Acet) | 0.044 | 0.4 | <LOQ | 5000 |
| Isopropanol (2-Pro) | 1.16 | 3.868 | ND | 5000 | Acetonitrile (Acetonit) | 0.888 | 2.952 | ND | 410 |
| Methylene Chloride (MetCh) | 0.04 | 0.4 | ND | 1 | Hexane (Hex) | 0.012 | 0.4 | ND | 290 |
| Ethyl Acetate (EthAc) | 0.032 | 0.4 | 150.9 | 5000 | Chloroform (Clo) | 0.028 | 0.4 | ND | 1 |
| Benzene (Ben) | 0.012 | 0.4 | ND | 1 | 1-2-Dichloroethane (12-Dich) | 0.024 | 0.4 | ND | 1 |
| Heptane (Hep) | 0.012 | 0.4 | ND | 5000 | Trichloroethylene (TriClEth) | 0.072 | 0.4 | ND | 1 |
| Toluene | 0.036 | 0.4 | ND | 890 | Xylenes (Xyl) | 0.012 | 0.4 | ND | 2170 |