QA Testing

California / other_product
cannabinoid,metal,microbial,mycotoxin,pesticide,residual,visual,water
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PharmLabs San Diego Certificate of Analysis
Sample Chocolate Bar - 20220809GR
Delta9 THC ND THCa ND Total THC (THCa * 0.877 + THC) ND Delta8 THC ND
Logo_coa
Sample ID  SD220817-008 (50547) Matrix   Edible
Distributor License   2022-R-1939322 Address   601 FAIRWAY DR Name   Green Roads
Sampled   - Received   Aug 16, 2022 Reported   Sep 06, 2022
Analyses executed   FP-NI Unit Mass (g)   48.475 Serving Size (g)   48.475

Laboratory note: The estimated concentration of the unknown peak in the sample is 0.39% | Currently PharmLabs laboratory can not confirm an unidentified peak in your chromatogram due to interference (only with highly concentrated D8 products) from which we believe to be either (+)d8-THC or d9-THC. At this time there are no reference standards available for (+)d8-THC. (+)d8-THC is a different compound from the main (-)d8-THC cannabinoid and, therefore, these two compounds may have different efficacies. Using the most advanced instruments and techniques available, the separation of (+)d8-THC and d9-THC is problematic for the scientific community as a whole. PharmLabs believes the unidentified peak to be a combination of (+)d8-THC and d9-THC with the majority, if not all, of the concentration being (+)d8-THC. Total (+/-) D8 Concentration is estimated to be 1.35% Note: 1 Chocolate bar per Package

CAN+ - Cannabinoids

Analyzed Aug 31, 2022  |  Instrument HPLC-VWD  | Method SOP-001
The expanded Uncertainty of the Cannabinoids analysis is approximately ± 7.81% at the 95% Confidence Level
Analyte   LOD
mg/g 		LOQ
mg/g 		Result
% 		Result
mg/g		 Result
mg/Serving		 Result
mg/Unit
Cannabidivarin (CBDv)   0.039 0.16 ND ND ND ND
Cannabidibutol (CBDb)   0.011 0.03 NT NT NT NT
Cannabidiolic Acid (CBDA)   0.033 0.16 ND ND ND ND
Cannabigerol Acid (CBGA)   0.033 0.16 ND ND ND ND
Cannabigerol (CBG)   0.048 0.16 ND ND ND ND
Cannabidiol (CBD)   0.069 0.229 0.43 4.32 209.51 209.51
Tetrahydrocannabivarin (THCV)   0.049 0.16 ND ND ND ND
Cannabinol (CBN)   0.047 0.16 ND ND ND ND
Tetrahydrocannabinol (Δ9-THC)   0.092 0.307 ND ND ND ND
Δ8-tetrahydrocannabinol (Δ8-THC)   0.044 0.16 ND ND ND ND
Cannabicyclol (CBL)   0.0012 0.16 ND ND ND ND
Cannabichromene (CBC)   0.13 0.432 ND ND ND ND
Tetrahydrocannabinolic Acid (THCA)   0.117 0.389 ND ND ND ND
Total THC ( THCa * 0.877 + Δ9THC )       ND ND ND ND
Total THC + Δ8THC ( THCa * 0.877 + Δ9THC + Δ8THC )       ND ND ND ND
Total CBD ( CBDa * 0.877 + CBD )       0.43 4.32 209.51 209.51
Total CBG ( CBGa * 0.877 + CBG )       ND ND ND ND
Total Cannabinoids Analyzed       0.43 4.32 209.51 209.51

HME - Heavy Metals

Analyzed Aug 19, 2022  |  Instrument ICP/MSMS  | Method SOP-005
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Arsenic (As) 0.0009 0.0027 ND 1.5
Cadmium (Cd) 0.0005 0.0015 ND 0.5
Mercury (Hg) 0.0058 0.0174 ND 3
Lead (Pb) 0.0006 0.0018 ND 0.5
Nickel (Ni) 6.0e-05 0.0002 NT

MIBNIG - Microbial

Analyzed Aug 18, 2022  |  Instrument Plating  | Method SOP-007
Analyte LOD
CFU/g 		LOQ
CFU/g 		Result
CFU/g 		Limit
CFU/g
Shiga toxin-producing Escherichia Coli 1.0 1.0 ND 1
Salmonella spp. 1.0 1.0 ND 1

MTO - Mycotoxin

Analyzed Aug 31, 2022  |  Instrument LC/MSMS  | Method SOP-004
Analyte LOD
ug/kg 		LOQ
ug/kg 		Result
ug/kg 		Limit
ug/kg 		Analyte LOD
ug/kg 		LOQ
ug/kg 		Result
ug/kg 		Limit
ug/kg
Ochratoxin A 5.0 20.0 ND 20 Aflatoxin B1 2.5 5.0 ND -
Aflatoxin B2 2.5 5.0 ND - Aflatoxin G1 2.5 5.0 ND -
Aflatoxin G2 2.5 5.0 ND - Total Aflatoxins 10.0 20.0 ND 20

PES - Pesticides

Analyzed Aug 31, 2022  |  Instrument LC/MSMS GC/MSMS  | Method SOP-003
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Aldicarb 0.01 0.02 ND Carbofuran 0.01 0.02 ND
Dimethoate 0.01 0.02 ND Etofenprox 0.02 0.1 ND
Fenoxycarb 0.01 0.02 ND Thiachloprid 0.01 0.02 ND
Daminozide 0.01 0.03 ND Dichlorvos 0.02 0.07 ND
Imazalil 0.02 0.07 ND Methiocarb 0.01 0.02 ND
Spiroxamine 0.01 0.02 ND Coumaphos 0.01 0.02 ND
Fipronil 0.01 0.1 ND Paclobutrazol 0.01 0.03 ND
Chlorpyrifos 0.01 0.04 ND Ethoprophos (Prophos) 0.01 0.02 ND
Baygon (Propoxur) 0.01 0.02 ND Chlordane 0.04 0.1 ND
Chlorfenapyr 0.03 0.1 ND Methyl Parathion 0.02 0.1 ND
Mevinphos 0.03 0.08 ND Abamectin 0.03 0.08 ND
Acephate 0.02 0.05 ND Acetamiprid 0.01 0.05 ND
Azoxystrobin 0.01 0.02 ND Bifenazate 0.01 0.05 ND
Bifenthrin 0.02 0.35 ND Boscalid 0.01 0.03 ND
Carbaryl 0.01 0.02 ND Chlorantraniliprole 0.01 0.04 ND
Clofentezine 0.01 0.03 ND Diazinon 0.01 0.02 ND
Dimethomorph 0.02 0.06 ND Etoxazole 0.01 0.05 ND
Fenpyroximate 0.02 0.1 ND Flonicamid 0.01 0.02 ND
Fludioxonil 0.01 0.05 ND Hexythiazox 0.01 0.03 ND
Imidacloprid 0.01 0.05 ND Kresoxim-methyl 0.01 0.03 ND
Malathion 0.01 0.05 ND Metalaxyl 0.01 0.02 ND
Methomyl 0.02 0.05 ND Myclobutanil 0.02 0.07 ND
Naled 0.01 0.02 ND Oxamyl 0.01 0.02 ND
Permethrin 0.01 0.02 ND Phosmet 0.01 0.02 ND
Piperonyl Butoxide 0.02 0.06 ND Propiconazole 0.03 0.08 ND
Prallethrin 0.02 0.05 ND Pyrethrin 0.05 0.41 ND
Pyridaben 0.02 0.07 ND Spinosad A 0.01 0.05 ND
Spinosad D 0.01 0.05 ND Spiromesifen 0.02 0.06 ND
Spirotetramat 0.01 0.02 ND Tebuconazole 0.01 0.02 ND
Thiamethoxam 0.01 0.02 ND Trifloxystrobin 0.01 0.02 ND
Acequinocyl 0.02 0.09 ND Captan 0.01 0.02 ND
Cypermethrin 0.02 0.1 ND Cyfluthrin 0.04 0.1 ND
Fenhexamid 0.02 0.07 ND Spinetoram J,L 0.02 0.07 ND
Pentachloronitrobenzene 0.01 0.1 ND Chlormequat Chloride 0.02 0.1 NT

RES - Residual Solvents

Analyzed Aug 19, 2022  |  Instrument GC/FID with Headspace Analyzer  | Method SOP-006
Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g		 Analyte LOD
ug/g 		LOQ
ug/g 		Result
ug/g 		Limit
ug/g
Propane (Prop) 0.044 0.4 ND 5000 Butane (But) 0.02 0.4 ND 5000
Methanol (Metha) 1.176 3.92 77.7 3000 Ethylene Oxide (EthOx) 0.08 0.4 ND 1
Pentane (Pen) 0.024 0.4 ND 5000 Ethanol (Ethan) 0.048 0.4 ND 5000
Ethyl Ether (EthEt) 0.036 0.4 ND 5000 Acetone (Acet) 0.044 0.4 ND 5000
Isopropanol (2-Pro) 1.16 3.868 ND 5000 Acetonitrile (Acetonit) 0.888 2.952 ND 410
Methylene Chloride (MetCh) 0.04 0.4 ND 1 Hexane (Hex) 0.012 0.4 ND 290
Ethyl Acetate (EthAc) 0.032 0.4 ND 5000 Chloroform (Clo) 0.028 0.4 ND 1
Benzene (Ben) 0.012 0.4 ND 1 1-2-Dichloroethane (12-Dich) 0.024 0.4 ND 1
Heptane (Hep) 0.012 0.4 ND 5000 Trichloroethylene (TriClEth) 0.072 0.4 ND 1
Toluene 0.036 0.4 ND 890 Xylenes (Xyl) 0.012 0.4 ND 2170

FVI - Filth & Foreign Material Inspection

Analyzed Aug 17, 2022  |  Instrument Microscope  | Method SOP-010
Analyte / Limit Result
 Analyte / Limit Result
> 1/4 of the total sample area
covered by sand, soil, cinders, or dirt 		ND > 1/4 of the total sample area
covered by mold 		ND
> 1 insect fragment, 1 hair, or 1 count
mammalian excreta per 3g 		ND > 1/4 of the total sample area
covered by an imbedded foreign material 		ND

MWA - Moisture Content & Water Activity

Analyzed Aug 22, 2022  |  Instrument Chilled-mirror Dewpoint and Capacitance  | Method SOP-008
Analyte LOD
aw 		LOQ
aw 		Result
 Limit Analyte LOD
% M/w 		LOQ
% M/w 		Result
 Limit
Water Activity (WA) 0.03 0.03 0.42 aw 0.85 aw Moisture (Moi) 0.0 0.0 5.8 % Mw 13 % Mw